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Beilstein J. Org. Chem. 2010, 6, 848–858, doi:10.3762/bjoc.6.100
Graphical Abstract
Scheme 1: Different types of 1-D and 2-D HBN forming supramolecular synthons.
Scheme 2: Salts studied in the present report.
Figure 1: Photomicrographs of the organogels (from left to right: nitrobenzene gel of DBUAMC 3; 1,2-dichlorob...
Figure 2: DSC of a 4.0 wt % 1,2-dichlorobenzene gel of DBAMC 6.
Figure 3: Left – Tgel vs [gelator] plot; right – semilog plot of mole fraction of the gelators against 1/T; 1...
Figure 4: SEM micrographs of the xerogels. (a) & (b) 0.5 wt % 1,2-dichlorobenzene gel of DBAMC 6; (c) 0.8 wt ...
Figure 5: Crystal structure illustration of DBUAMC 3; 3-D hydrogen bonded network; only one part of the disor...
Figure 6: Crystal structure illustrations of DBAMC 6; top – propagation 1-D network involving ammonium and ca...
Figure 7: Illustration of crystal structure of DCHADC 1; top – 1-D hydrogen bonded zigzag chain displaying SA...
Figure 8: PXRD patterns of salts 3, 6 and 1 under various conditions.